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Phenergan gel (2%) was added. The mixture stirred for 30 min at room temperature. The reaction was quenched with 40 N HCl. The filtrate was filtered and dried over Na 2 SO 4, filtered and concentrated under reduced pressure. The oil was purified by column chromatography eluting with hexane-ethyl acetate (20:70) providing a residue of 10.0 g 2-amino-2,5-dimethyl-4-phenylpropane sulfone (PPS-PN). The reaction mixture contained PPS-PN and isopropyl alcohol at a volume of 20% (v/v). The mixture was stirred at room temperature for 5 min. The reaction mixture was cooled to 0° C. and the mixture was stirred for a further 10 min. The mixture was quenched with NH 4 Cl and Generika viagra online kaufen the methanol was removed. solvent evaporated leaving a residue of 5.9 g 2-aminobipropane sulfone (PPS-PN). The reaction mixture was then concentrated under reduced pressure and the residue was purified by column chromatography eluting with hexane-ethyl acetate (20:70) providing a residue of 4.5 g 2-aminobipropane sulfone (PPS-PN). The following procedure was carried out to recover the two isomers of 2-amino-2,5-dimethyl-4-phenylpropane sulfone using a 2-amino-diphenyl-piperazine derivative. This procedure was carried out as described in Example 1 for preparing isomer 1. 4.8.2. Synthesis of 4-Amino-2-nitro-1-phenylcyclohexanone (N-benzoxazol-1-yl-2-pyrrolidinol) Synthesis of 4-bromo-2-nitro-1-phenylcyclohexanone can i buy phenergan over the counter in uk (N-benzoxazol-1-yl-2-pyrrolidinol) from 4-cyano-4-nitro-5-phenyl-pyrrolidinone (Table 1) was carried out using 4-cyano-4-nitro-5-phenyl-pyrrolidinone (7.6 g) as the starting material. The 2-nitro-4-cyano group was removed by a reduction with diethylenediamine in CH 2 Cl (0.025 g, 10.0 mmol) and the residue was purified by Buying indomethacin column chromatography eluting with hexane-ethyl acetate (20:70) providing a residue of 0.7 g 2-nitro-4-cyano-5-phenyl-pyrrolidinol (N-benzoxazol-1-yl-2-pyrrolidinol). 4.8.3. Synthesis of 4-Amino-2-nitro-1-phenylcyclohexanone (N-benzoxazol-1-yl-2-pyrrolidinol) The reaction of 4-aminobipropyl-2-nitro-1-phenylcyclohexanone (1) with diethylenediamine (0.01 g, 10.0 mmol) provided the 4-cyano derivative as shown in Table 1. N-benzoxazol-1-yl-2-pyrrolidinol (1) was prepared by reacting 4-aminobipropyl-2-nitro-1-phenylcyclohexanone with diethylenediamine (0.01 g, 8.5 mmol) in CH 2 Cl (5:2) anhydrous methanol (10 ml, 18%) for 8 hours at -10° C. and cooling to After -10° C., the solution was cooled to -5° C. and washed with water. The solution was concentrated to give a solid residue (1.0 g, 58%). 4.8.4. Synthesis of 4-a-aminobipropyl-2-nitro-1-phenylcyclohexanone (N-benzoxazol-1-yl-2-pyrrolidinol) The reaction of 4-aminobipropyl-2-nitro-1-phenylcyclohexanone (2) with diethylenediamine (0.01 g, 10.0 mmol) provided the 4-cyano derivative as shown in Table 1. N-benzoxazol-1-yl-2-pyrrolidinol (2)

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This press was recovered from an external storage area.  The press, luckily, had not been stored outside for long and was not heavily bitten with rust, so the fine casting details were in good condition.  The bed and platen needed complete re-machining to provide good clean printing surfaces as these surfaces had become damaged.  A number of parts were missing, including the brass bearings and some hardened linkage.  The press was brought back to our works and completely rebuilt and the missing parts replaced. 

A Tympan inner, outer, frisket and hinge were manufactured and fitted to the bed.  The press was final assembled in our works and proofed before being painted (3 coats of gloss black) and final polished.  The press now stands in the main print area at the West Yorkshire Printworkshop, where it is regularly used.