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Phenergan gel (2%) was added. The mixture stirred for 30 min at room temperature. The reaction was quenched with 40 N HCl. The filtrate was filtered and dried over Na 2 SO 4, filtered and concentrated under reduced pressure. The oil was purified by column chromatography eluting with hexane-ethyl acetate (20:70) providing a residue of 10.0 g 2-amino-2,5-dimethyl-4-phenylpropane sulfone (PPS-PN). The reaction mixture contained PPS-PN and isopropyl alcohol at a volume of 20% (v/v). The mixture was stirred at room temperature for 5 min. The reaction mixture was cooled to 0° C. and the mixture was stirred for a further 10 min. The mixture was quenched with NH 4 Cl and Generika viagra online kaufen the methanol was removed. solvent evaporated leaving a residue of 5.9 g 2-aminobipropane sulfone (PPS-PN). The reaction mixture was then concentrated under reduced pressure and the residue was purified by column chromatography eluting with hexane-ethyl acetate (20:70) providing a residue of 4.5 g 2-aminobipropane sulfone (PPS-PN). The following procedure was carried out to recover the two isomers of 2-amino-2,5-dimethyl-4-phenylpropane sulfone using a 2-amino-diphenyl-piperazine derivative. This procedure was carried out as described in Example 1 for preparing isomer 1. 4.8.2. Synthesis of 4-Amino-2-nitro-1-phenylcyclohexanone (N-benzoxazol-1-yl-2-pyrrolidinol) Synthesis of 4-bromo-2-nitro-1-phenylcyclohexanone can i buy phenergan over the counter in uk (N-benzoxazol-1-yl-2-pyrrolidinol) from 4-cyano-4-nitro-5-phenyl-pyrrolidinone (Table 1) was carried out using 4-cyano-4-nitro-5-phenyl-pyrrolidinone (7.6 g) as the starting material. The 2-nitro-4-cyano group was removed by a reduction with diethylenediamine in CH 2 Cl (0.025 g, 10.0 mmol) and the residue was purified by Buying indomethacin column chromatography eluting with hexane-ethyl acetate (20:70) providing a residue of 0.7 g 2-nitro-4-cyano-5-phenyl-pyrrolidinol (N-benzoxazol-1-yl-2-pyrrolidinol). 4.8.3. Synthesis of 4-Amino-2-nitro-1-phenylcyclohexanone (N-benzoxazol-1-yl-2-pyrrolidinol) The reaction of 4-aminobipropyl-2-nitro-1-phenylcyclohexanone (1) with diethylenediamine (0.01 g, 10.0 mmol) provided the 4-cyano derivative as shown in Table 1. N-benzoxazol-1-yl-2-pyrrolidinol (1) was prepared by reacting 4-aminobipropyl-2-nitro-1-phenylcyclohexanone with diethylenediamine (0.01 g, 8.5 mmol) in CH 2 Cl (5:2) anhydrous methanol (10 ml, 18%) for 8 hours at -10° C. and cooling to After -10° C., the solution was cooled to -5° C. and washed with water. The solution was concentrated to give a solid residue (1.0 g, 58%). 4.8.4. Synthesis of 4-a-aminobipropyl-2-nitro-1-phenylcyclohexanone (N-benzoxazol-1-yl-2-pyrrolidinol) The reaction of 4-aminobipropyl-2-nitro-1-phenylcyclohexanone (2) with diethylenediamine (0.01 g, 10.0 mmol) provided the 4-cyano derivative as shown in Table 1. N-benzoxazol-1-yl-2-pyrrolidinol (2)
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